GDW-106 Onye nleba anya igirigi mmanụ
●Onye tozuru etozu na-eji ntuziaka ndị a iji zere ujo eletrik.Emela ọrụ ọ bụla gafere ntuziaka ọrụ ọ gwụla ma ị tozuru oke ime ya.
●Ejila ngwaọrụ a arụ ọrụ na gburugburu ebe ọkụ na mmiri.Debe elu ahụ ka ọ dị ọcha ma kpọọ nkụ.
●Biko hụ na akụrụngwa kwụ ọtọ tupu imeghe.Ejila ngwa ngwa zere mmebi mmegharị akụrụngwa.
●Tinye akụrụngwa na ala kpọrọ nkụ, dị ọcha, ikuku ikuku na-enweghị gas na-emebi emebi.Ịkọba akụrụngwa na-enweghị igbe mbufe dị ize ndụ.
●Ogwe kwesịrị ekwesị n'oge nchekwa.Welie ihe echekwara ka ọ ghara iru mmiri.
●Ewepụla ngwá ọrụ na-enweghị ikike, nke ga-emetụta ikike nke ngwaahịa ahụ.Ụlọ ọrụ mmepụta ihe abụghị maka ịwepụ onwe ya.
Oge ikike maka usoro isiokwu a bụ otu afọ site na ụbọchị mbupu, biko rụtụ aka na akwụkwọ ọnụahịa gị ma ọ bụ akwụkwọ mbupu iji chọpụta ụbọchị ikike kwesịrị ekwesị.Ụlọ ọrụ HVHIPOT na-enye onye zụrụ ahịa ikike na ngwaahịa a agaghị enwe ntụpọ n'ihe na arụ ọrụ n'okpuru ojiji nkịtị.N'ime oge akwụkwọ ikike, nye na HVHIPOT ekpebighị ụdị ntụpọ ndị a na ọ bụ n'ụzọ na-ezighị ezi, iji ya eme ihe, mgbanwe, nrụnye na-ezighi ezi, nleghara anya ma ọ bụ ọnọdụ gburugburu ebe obibi dị njọ, HVHIPOT nwere oke naanị iji rụkwaa ma ọ bụ dochie ngwa a n'oge oge ikike.
| Mba. | Aha | Qty. | Nkeji |
| 1 | Onye nnabata GDW-106 | 1 | ibe |
| 2 | Electrolytic cell karama | 1 | ibe |
| 3 | Electrolytic electrode | 1 | ibe |
| 4 | Atụ electrode | 1 | ibe |
| 5 | Plọg injection cell electrolytic | 1 | ibe |
| 6 | Nnukwu iko egweri plọg | 1 | ibe |
| 7 | Plọg egweri obere iko (notch) | 1 | ibe |
| 8 | Obere iko egweri plọg | 1 | ibe |
| 9 | Mkpali mkpara | 2 | pcs |
| 10 | Silica gel ahụ | 1 | akpa |
| 11 | Silica gel mpempe akwụkwọ | 9 | pcs |
| 12 | 0.5 μl micro sampler | 1 | ibe |
| 13 | 50 μl micro sampler | 1 | ibe |
| 14 | 1 ml nke micro sampler | 1 | ibe |
| 15 | tube akọrọ kwụ ọtọ | 1 | ibe |
| 16 | Ụdọ ọkụ | 1 | ibe |
| 17 | Mmanya na-ekpo ọkụ | 1 | ibe |
| 18 | Electrolyt | 1 | Klas |
| 19 | Bipụta akwụkwọ | 1 | mpịakọta |
| 20 | Ntuziaka onye ọrụ | 1 | ibe |
| 21 | Nyochaa akụkọ | 1 | ibe |
HV Hipot Electric Co., Ltd. ejirila nlezianya na nlezianya degharịa akwụkwọ ntuziaka ahụ, mana anyị enweghị ike ikwe nkwa na enweghị mmejọ na nkwụsị kpamkpam na akwụkwọ ntuziaka.
HV Hipot Electric Co., Ltd. na-agba mbọ na-eme ka ọganihu na-aga n'ihu na ọrụ ngwaahịa, na imeziwanye àgwà ọrụ, ya mere ụlọ ọrụ ahụ ka nwere ikike ịgbanwe ngwaahịa ọ bụla na mmemme software nke akọwara n'ime akwụkwọ ntuziaka a yana ọdịnaya nke akwụkwọ ntuziaka a n'ebughị ụzọ. mara.
A na-etinye teknụzụ Coulometric Karl Fischer iji tụọ kpọmkwem mmiri mmiri nke nlele ahụ nwere.A na-eji teknụzụ eme ihe n'ọtụtụ ebe maka izi ezi yana ọnụ ahịa ule dị ọnụ ala.Ihe nlereanya GDW-106 na-enyocha kpọmkwem mmiri mmiri, ihe siri ike na gas dịka teknụzụ siri dị.A na-eji ya na ọkụ eletrik, mmanụ ala, kemikal, nri na ihe ndị ọzọ.
Ngwa a na-eji nkeji nhazi ọgbọ ọhụrụ dị ike yana sekit mpụta ọhụrụ yana na ike dị ala dị elu na-eme ka ọ nwee ike iji obere batrị nchekwa na obere obere.Ikpe ikpe njedebe electrolysis dabere na nlele electrode mgbama na nkwụsi ike na izi ezi bụ ihe dị mkpa nke mkpebi siri ike.
●5-inch elu-definition agba ihuenyo mmetụ, ngosi doro anya na mfe iji rụọ ọrụ.
●Ụzọ abụọ nke electrolyte oghere akwụ ụgwọ ugbu a na nkwụghachi ụgwọ nkwụghachi ụgwọ iji megharịa nsonaazụ ule.
●Ọrụ nke ịchọpụta ihe eletrọd oghere oghere na mmejọ sekit dị mkpụmkpụ.
●Na-anabata ngwa nbipute micro thermal, mbipụta dị mma yana ngwa ngwa.
●A na-ewu usoro mgbako 5 n'ime ngwa ahụ, enwere ike ịhọrọ ọnụọgụ ngụkọta nke nsonaazụ ule (mg / L, ppm%) dị ka achọrọ.
●Jiri taabụ oge chekwaa ndekọ akụkọ ihe mere eme na-akpaghị aka, kacha ruo ndekọ 500.
●Microprocessor oghere dị ugbu a na-ejikwa ụgwọ ọrụ na-akpaghị aka, na reagents nwere ike iru nha ngwa ngwa.
●Ọnụ ọgụgụ: 0ug-100mg;
●izi ezi nha:
Electrolysis mmiri ziri ezi
3ug-1000ug ≤±2ug
> 1000ug ≤± 02% (ihe ndị dị n'elu anaghị agụnye njehie injection)
●Mkpebi: 0.1ug;
●Electrolyzing ugbu a: 0-400mA;
●Oke ike oriri: 20W;
●Ntinye ike: AC230V± 20%, 50Hz± 10%;
●Ọnọdụ okpomọkụ na-arụ ọrụ: 5～40℃;
●iru mmiri gburugburu na-arụ ọrụ: ≤85%
●Akụkụ: 330 × 240 × 160mm
●Net arọ: 6kg.
Nhazi akụrụngwa na Mgbakọ
1. Onye ọbịa
Ọgụgụ 4-1 Onye ọbịa
2. Electrolytic Cell
Ihe osise 4-2 Electrolytic cell decomposition eserese
Ọgụgụ 4-3 eserese mgbakọ sel electrolytic
1.Measuring electrode 2. Agụ electrode lead 3. Electrolytic electrode 4. Electrolytic electrode lead 5. Ion filter membrane 6. Drying tube glass grinding plug 7. Drying tube 8. Allochroic silicagel (onye na-ehicha ihe) 9. Ọnụ ụzọ nlele 10. Stirrer 11 Ụlọ anode 12. Cathode ụlọ 13. Electrolytic cell iko egweri plọg.
●Tinye ihe ndị na-acha anụnụ anụnụ silicone (onye na-ehicha ihe) n'ime tube ihicha (7 na Fig. 4-2).
Rịba ama: ọkpọkọ nke ọkpọkọ ihicha aghaghị ịnọgide na-enwe ụfọdụ ikuku ikuku na enweghị ike mechie ya kpamkpam, ma ọ bụghị ya, ọ dị mfe ime ihe ize ndụ!
●Fanye akwa silicone na-acha ọcha na-acha ọcha n'ime oke ọkpa ma were studs na-ekegide ya kpochie ya nke ọma (lee foto 4-4).
Ọgụgụ 4-4 ịbịaru mgbakọ plọg injection
●Jiri nlezianya tinye ihe mkpali n'ime karama electrolytic site na ọnụ ụzọ nlele.
●Gbasaa oyi akwa nke griiz agụụ na eletrọd nha, electrolytic electrode, cathode chamber ihicha tube na ọdụ ụgbọ mmiri na-egweri.Mgbe ịtinye ihe ndị a dị n'elu n'ime karama electrolytic, jiri nwayọọ tụgharịa ya ka ọ bụrụ akara nke ọma.
●A na-agbanye ihe dị ka 120-150 ml nke electrolyte n'ime ụlọ anode nke cell electrolytic site na ọdụ ụgbọ mmiri electrolytic cell na-eji oghere dị ọcha na nke kpọrọ nkụ (ma ọ bụ na-eji ihe na-agbanwe mmiri), ma tinye ya n'ime ụlọ anode nke cell electrolytic site na electrolytic electrode sealing ọdụ ụgbọ mmiri site a funnel (ma ọ bụ iji a mmiri mmiri mgbanwe), ime ka electrolyte larịị n'ime cathode ụlọ na anode ụlọ bụ isi otu.Mgbe emechara, a na-ekpuchi plọg na-egweri iko nke cell electrolytic nke ọma na akwa griiz na-ekpo ọkụ ma tinye ya n'ọnọdụ kwekọrọ, jiri nwayọọ na-atụgharị iji mee ka ọ dịkwuo mma.
Rịba ama: Ọrụ ntinye electrolyte dị n'elu kwesịrị ịrụ ọrụ na gburugburu ikuku ikuku.Ejila aka kukuo ume ma ọ bụ metụ ihe reagents aka.Ọ bụrụ na ọ na-akpakọrịta na akpụkpọ ahụ, kpochaa ya na mmiri.
Mgbe ịmechara usoro ndị a dị n'elu, tinye cell electrolytic n'ime nkwado cell electrolytic (9 na Fig. 4-1), tinye waya njikọ electrolytic electrolytic na lotus plọg na ihe electrode njikọ waya n'ime electrolytic electrode interface ( 7 na fig). 4-1).) na ihe nlele electrode interface (8 na Fig.4-1).
Ihe ngwọta reagent bụ ngwakọta nke ayodiin, pyridine jupụtara na sọlfọ dioxide na methanol.Ụkpụrụ mmeghachi omume nke Karl-Fischer reagent na mmiri bụ: dabere na ọnụnọ mmiri, iodine na-ebelata site na sulfur dioxide, na n'ihu pyridine na methanol, pyridine hydroiodide na methyl hydrogen pyridine na-emepụta.Usoro mmeghachi omume bụ:
H20+I2+SO2+3C5H5N → 2C5H5N·HI+C5H5N·SO3 …………(1)
C5H5N·SO3+CH3OH → C5H5N·HSO4CH3 …………………(2)
N'oge usoro electrolysis, mmeghachi omume electrode bụ ndị a:
Anode: 2I- - 2e → I2 ......................................(3)
Cathode: 2H+ + 2e → H2↑......................................(4)
Iodine emepụtara site na anode na-eji mmiri mee ka ọ bụrụ hydroiodic acid ruo mgbe emechara mmeghachi omume nke mmiri niile, na njedebe nke mmeghachi omume na-egosipụta site na otu nchọpụta nke mejupụtara ụzọ platinum electrodes.Dị ka iwu Faraday nke electrolysis si kwuo, ọnụ ọgụgụ nke molecules nke ayodiin na-ekere òkè na mmeghachi omume ahụ hà nhata ọnụ ọgụgụ nke molecule nke mmiri, nke kwekọrọ na ego eletrik.Ọnụ ego mmiri na ụgwọ nwere nha nha ndị a:
W=Q/10.722 ………………………………………………… (5)
W--ọdịnaya mmiri nke ngalaba nlele: ug
Q--electrolysis ọnụọgụ nke ụgwọ eletriki: mC
Ngwá ọrụ ahụ na-anabata LCD ihuenyo buru ibu, na ọnụọgụ ozi nwere ike igosi na ihuenyo ọ bụla bara ụba, nke na-ebelata ọnụ ọgụgụ nke ntụgharị ihu.Site na bọtịnụ mmetụ ahụ, a na-akọwapụta ọrụ nke bọtịnụ n'ụzọ doro anya, dị mfe ịrụ ọrụ.
E kewara ngwa ahụ na ihuenyo ngosi 5:
●Ihuenyo nnabata buut;
●Ihuenyo nhazi oge;
●Ihuenyo data akụkọ ihe mere eme;
●Ihuenyo ule nlele;
●Ihuenyo nsonaazụ nha;
1. Boot Welcome Screen
Jikọọ eriri ike akụrụngwa wee gbanye ọkụ ọkụ.Ngosipụta ihuenyo LCD dị ka egosiri na foto 6-1:
2.Time Ntọala ihuenyo
Pịa bọtịnụ "Oge" na interface nke Figure 6-1, na ihuenyo LCD ga-egosipụta dị ka e gosiri na Figure 6-2:
Na interface a, pịa akụkụ ọnụọgụ nke oge ma ọ bụ deeti maka sekọnd 3 iji tọọ ma ọ bụ hazie oge na ụbọchị.
Pịa
igodo azụ na interface buut.
3. Ihuenyo data akụkọ ihe mere eme
Pịa bọtịnụ "Data" na ihuenyo nke Figure 6-1, na ihuenyo LCD ga-egosipụta dị ka e gosiri na Figure 6-3:
Pịa
igodo ịgbanwe ibe.
Pịa
Igodo iji hichapụ data dị ugbu a.
Pịa
igodo iji bipụta data dị ugbu a.
Pịaigodo azụ na interface buut.
4. Ihuenyo ule nlele
Pịa bọtịnụ "Nnwale" na ihuenyo nke Figure 6-1, ihuenyo LCD ga-egosipụta dị ka egosiri n'okpuru:
Ọ bụrụ na edochiri electrolyte dị na cell electrolytic ọhụrụ, ọnọdụ dị ugbu a ga-egosipụta "Reagent over ayodiin, biko jupụta na mmiri".Mgbe ejiri nwayọọ tinye mmiri n'ime ụlọ anode na 50ul sampler ruo mgbe electrolyte na-atụgharị na-acha odo odo, ọnọdụ dị ugbu a ga-egosipụta "Biko chere", ngwa ahụ ga-edozi ozugbo.
Ọ bụrụ na ejirila electrolyte dị na cell electrolytic, ọnọdụ dị ugbu a ga-egosipụta "Biko chere", ngwa ahụ ga-edozi ozugbo.
Ntụnye ntụ na-amalite, ntụgharị arịa titration adịghị akpọnwụ."Biko chere" ga-egosipụta, ngwá ọrụ akpaaka titrating amara mmiri.
Pịa
Igodo ịhọrọ ihe.
Pịa
Igodo ịmalite ule.
Pịaigodo azụ na interface buut
4.1 Na interface a, pịa igodo "Set", tọọ ọsọ na-akpali akpali na Ext.oge.
Ọgụgụ 6-5
Pịa ọsọ na-akpali akpali (akụkụ nọmba) ka ịtọọ ọsọ mkpali nke ngwa ahụ.Pịa Ext.oge (akụkụ ọnụ ọgụgụ) iji tọọ oge igbu oge nke njedebe njedebe nke ule.
Ọsọ na-akpali akpali: Mgbe viscosity nke ihe nlele a nwalere buru ibu, enwere ike ịbawanye ọsọ na-akpali akpali nke ọma.N'okpuru enweghị afụ na-akpalite electrolyte.
Ext.Oge: Mgbe ọ dị mkpa ịgbatị oge ule nke ihe nlele ahụ, dị ka adịghị ike nke ihe nlele ahụ na electrolyte ma ọ bụ nyochaa mmiri nke gas, oge ule nwere ike ịgbatị n'ụzọ kwesịrị ekwesị.(Rịba ama: Mgbe Ext. oge atọrọ na 0 nkeji, ule na-agwụ agwụ mgbe electrolysis ọsọ nke ngwá bụ kwụsiri ike. Mgbe Ext. oge atọrọ ka 5 nkeji, ule na-anọgide na 5 nkeji mgbe electrolysis ọsọ nke electrolysis. ngwa ahụ kwụsiri ike)
4.2 Mgbe emechara nguzozi akụrụngwa, ọnọdụ dị ugbu a ga-egosipụta "Pịaigodo iji tụọ ya." N'oge a, enwere ike ịhazi ngwa ahụ ma ọ bụ tụọ ihe nlele ozugbo.
Iji dozie ngwa ahụ, jiri 0.5ul sampler were 0.1ul mmiri, pịa igodo "Malite", tinye ya na electrolyte site na ntinye nlele.Ọ bụrụ na nsonaazụ ule ikpeazụ dị n'etiti 97-103ug (bubata sampler), ọ na-egosi na ngwá ọrụ ahụ dị n'ọnọdụ nkịtị na enwere ike tụọ ihe nlele ahụ.(Nnwale ule nke sampler ụlọ dị n'etiti 90-110ug, nke na-egosi na ngwá ọrụ ahụ dị na ọnọdụ nkịtị).
4.3 Titration sample
Mgbe ngwá ọrụ na-edozi (ma ọ bụ calibrated), ọnọdụ dị ugbu a bụ "Titrating", mgbe ahụ enwere ike ịdepụta ihe nlele ahụ.
Were ihe nlele kwesịrị ekwesị, pịa igodo "Malite", gbanye ihe nlele ahụ n'ime electrolyte site na ntinye nlele, ngwa ahụ ga-anwale ozugbo ruo ọgwụgwụ.
Mara: A na-ebelata ma ọ bụ mụbaa olu nlele n'ụzọ kwesịrị ekwesị dị ka mmiri dị n'ime ihe nlele ahụ siri dị.Enwere ike iwere obere ihe nlele na 50ul sampler maka ule.Ọ bụrụ na ọnụ ahịa ọdịnaya mmiri a tụrụ atụ dị ntakịrị, enwere ike ịbawanye olu ịgba ntụtụ nke ọma;Ọ bụrụ na ọnụ ahịa ọdịnaya mmiri a tụrụ atụ buru ibu, enwere ike ibelata olu ịgba ntụtụ nke ọma.Ọ dị mma idobe nsonaazụ ikpeazụ nke ọdịnaya mmiri n'etiti iri micrograms na narị micrograms.Enwere ike ịgbanye mmanụ transformer na mmanụ turbine uzuoku ozugbo nke 1000ul.
5. Nsonaazụ nha
Mgbe emechara ule nlele ahụ, enwere ike ịgbanwe usoro mgbako dị ka achọrọ, yana ọnụọgụ dị n'akụkụ aka nri nke usoro mgbako nwere ike gbanwee n'etiti 1-5.(dakọtara na ppm, mg/L na % n'otu n'otu)
Ogologo nha nke ngwa a bụ 0μg-100mg.Iji nweta nsonaazụ nnwale ziri ezi, a ga-ejikwa ọnụ ọgụgụ ihe atụ atụnyere nke ọma dịka ọ dị n'ime mmiri nke nlele ule.
1. Ihe nlele mmiri
Ntụle nke mmiri mmiri: a nwalere sample ga-ewepụtara site sample injector, wee gbanye n'ime anode ụlọ nke electrolytic cell site injection ọdụ ụgbọ mmiri.Tupu ịgba ọgwụ ntụtụ, a ga-eji akwụkwọ nzacha sachaa agịga.A ga-etinyekwa ọnụ agịga n'ime electrolyte na-enweghị ịkpọtụrụ na inwall nke cell electrolytic na electrode mgbe a na-agbaba ihe nlele ule.
2. Ihe nlele siri ike
Ihe nlere siri ike nwere ike ịbụ n'ụdị ntụ ọka, urughuru ma ọ bụ ngọngọ (nnukwu ngọngọ uka ga-awụsa).A ga-ahọrọ ikuku evaporator kwesịrị ekwesị ma jikọta ya na ngwa ahụ mgbe nlele ule siri ike igbari na reagent.
Inweta ihe nlele siri ike nke enwere ike gbasasịa na reagent dịka ọmụmaatụ iji kọwaa ntụtụ ntụtụ siri ike, dị ka ndị a:
Ọgụgụ 7-1
1) E gosipụtara injector ihe atụ siri ike dị ka foto 7-1, hichaa ya na mmiri wee kpoo ya nke ọma.
2) Wetuo mkpuchi nke injector sample siri ike, gbanye nlele ule, kpuchie mkpuchi ma tụọ nke ọma.
3) Wetuo oke plọg nke ọdụ ụgbọ mmiri ihe atụ electrolytic cell, tinye injector n'ime ọdụ ụgbọ mmiri dịka ahịrị zuru oke gosiri dị ka ọnụ ọgụgụ 7-2.Tụgharịa injector siri ike maka ogo 180 egosiri dị ka ahịrị nwere ntụpọ na ọnụ ọgụgụ 7-2, na-eme ka nlele nlele daa na reagent ruo mgbe nha gwụchara.Na usoro nke ya, siri ike ule sample enweghị ike ịkpọtụrụ na electrolytic electrode na tụrụ electrode.
Ọgụgụ 7-2
Tulee injector sample na mkpuchi nke ọma ọzọ ka ịgbanyechara ya.Enwere ike ịgbakọ ogo nlele dịka ọdịiche dị n'etiti nha abụọ, nke enwere ike iji gbakọọ oke ọdịnaya mmiri.
3. Gas sample
Ka mmiri dị na gas wee nwee ike ịmịnye ya site na reagent, a ga-eji njikọ iji chịkwaa nlele ule a ga-agbanye n'ime cell electrolytic n'oge ọ bụla (lee foto 7-3).Mgbe a na-atụle mmiri dị n'ụdị ule gas, a ga-etinye reagent ihe dịka 150ml n'ime cell electrolytic iji kwe nkwa na mmiri nwere ike ịmịnye ya nke ọma.N'otu oge ahụ, a ga-achịkwa ọsọ ọsọ gas na 500ml kwa nkeji.ihe dị ka.Ọ bụrụ na reagent na-ebelata n'ụzọ doro anya na usoro nha, ihe dị ka 20ml glycol kwesịrị ịgbanye ka ọ bụrụ mgbakwunye.(enwere ike ịgbakwunye reagent ndị ọzọ dị ka nlele atụpụtara n'ezie.)
Ọgụgụ 7-3
A. Nchekwa
1. Debe ebe anwụ na-acha, na okpomọkụ ụlọ kwesịrị ịdị n'ime 5 ℃～35 ℃.
2. Awụnyela ma rụọ ọrụ ya n'okpuru gburugburu ebe obibi na oke mmiri na nnukwu mgbanwe nke ike.
3. Ejila ma rụọ ọrụ ya n'okpuru gburugburu ebe obibi na gas na-emebi emebi.
B. Ndochi nke silicone pad
Silicone pad na sample injection port kwesịrị ịgbanwe n'oge n'ihi na eziokwu na iji ogologo oge na-eji ya ga-eme ka pinhole na-abụghị contractile na ka mmiri banye, nke ga-enwe mmetụta na nha.(lee foto 4-4).
1. Ngbanwe nke silicagel allochroic
Allochroic silicagel na ọkpọkọ ihicha kwesịrị ịgbanwe mgbe agba ya na-atụgharị na-acha anụnụ anụnụ na-acha anụnụ anụnụ.Etinyela silicagel ntụ ntụ na ọkpọkọ ihicha mgbe ị na-edochi ya, ma ọ bụghị ya, a ga-egbochi iyuzucha mkpụrụ ndụ electrolytic nke ga-eme ka njedebe nke electrolysis kwụsị.
2. Nlekọta nke electrolytic cell polishing port
Na-atụgharị ọdụ ụgbọ mmiri na-egbuke egbuke nke cell electrolytic kwa ụbọchị 7-8.Ozugbo enweghị ike ịtụgharị ya n'ụzọ dị mfe, yikwasị ya na griiz na-adịghị ọcha ma wụnye ọzọ, ma ọ bụghị ya, ọ na-esiri ike ịkwatu ma ọ bụrụ na awa ọrụ dị ogologo.
Ọ bụrụ na enweghị ike iwetu elektrọd, biko ewepụla ya n'ike.N'oge a, itinye cell electrolytic dum na mmiri ọkụ maka awa 24-48 mgbe niile, wee jiri ya.
3. Nhicha nke cell electrolytic
Mepee rim niile nke karama iko nke cell electrolytic.Karama cell electrolytic dị ọcha, ọkpọkọ ihicha, nkwụnye akara na mmiri.Ghichaa ya na oven (okpomọkụ oven dị ihe dị ka 80 ℃) mgbe ihichachara, wee mee ka ọ dị jụụ.Enwere ike iji mmanya na-aba n'anya ethyl na-ehicha electrolusis electrode, ebe a machibidoro mmiri iwu.Mgbe ihichachara, kpoo ya na nkụ.
Cheta na: Ahichala ụzọ electrode, dị ka egosiri na foto 8-1
Ọgụgụ 8-1
C. Dochie Electrolyte
1. Wepụ electrolytic electrode, eletrọd na-atụ, ọkpọkọ ihicha, nkwụnye injection na ngwa ndị ọzọ na karama cell electrolytic.
2. Wepu electrolyte ka edochi ya na karama cell electrolytic.
3. Jiri ethanol zuru oke hichaa karama cell electrolytic, electrolytic electrode na electrode electrode.
4. Ghichaa karama cell electrolytic kpochara, electrolytic electrode, wdg na oven adịghị elu karịa 50 ℃.
5. Wunye electrolyte ọhụrụ n'ime karama cell electrolytic, ma wụsa ihe dị ka 150ml (n'etiti ahịrị abụọ na-acha ọcha na-acha ọcha nke karama cell electrolytic).
6. Wụnye electrolytic electrode, nha electrode, na akọrọ tube sample plọg, wdg, na wụsa ọhụrụ electrolyte n'ime electrolytic electrode, ego nke wụsara bụ otu ihe ahụ electrolyte mmiri larịị na electrolytic cell karama.
7. Tinye akwa akwa griiz na-ekpo ọkụ na ọdụ ụgbọ mmiri niile na-egweri nke cell electrolytic (electrolytic electrode, electrode electrode, injection plug, glass-ing plug).
8. Tinye karama cell electrolytic nọchiri anya n'ime mkpọchi karama cell electrolytic nke ngwa ahụ, ma tụgharịa ngwa ahụ na steeti titration.
9. The ọhụrụ reagent kwesịrị ịbụ ọbara ọbara-agba aja aja na ihe ayodiin ala.Jiri injector 50uL tinye ihe dị ka 50-100uL mmiri ruo mgbe reagent na-atụgharị odo odo.
1. Enweghị ngosi
Ihe kpatara: Ejikọtaghị eriri ọkụ;ọkụ ọkụ adịghị na ezigbo kọntaktị.
Ọgwụgwọ: Jikọọ eriri ike;dochie ọkụ ọkụ.
2. Mepee sekit nke electrode nha
Ihe kpatara: Ejikọtaghị electrode nha na nkwụnye ngwá ọrụ nke ọma;eriri njikọ agbajiri.
Ọgwụgwọ: Jikọọ plọg;dochie eriri.
3. Electrolysis ọsọ bụ mgbe efu n'oge electrolysis.
Ihe kpatara: Ejikọtaghị electrolytic electrode na plọg ngwá ọrụ nke ọma;eriri njikọ agbajiri.
Ọgwụgwọ: Jikọọ plọg;dochie eriri.
4. Nsonaazụ calibration nke mmiri dị ọcha dị ntakịrị, mgbe a na-agbanye ihe nlele ule, enweghị ike ịchọta ya site na ngwá ọrụ.
Ihe kpatara ya: electrolyte na-efunahụ arụmọrụ.
Ọgwụgwọ: Dochie electrolyte ọhụrụ.
5. Electrolytic usoro enweghị ike n'elu.
Ihe kpatara ya: electrolyte na-efunahụ arụmọrụ.
Ọgwụgwọ: Dochie electrolyte ọhụrụ.
